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Engineering Notes ....

 
     
  Engineering Evaluation  
     
 

Graphite Furnaces Versus Refractory Metal Furnaces

for Powder Metal Processing Techniques

 
     
 

The use of powder metal for the creation of highly engineered and sophisticated shapes with minimum secondary work has become very popular for both low and high volume production. The use of Powder Metal Technology requires a means to remove the binding material used to hold the metal powder together and densify the metal alloy from the powder. These requirements are fulfilled with one or two furnaces, sometimes augmented by a solvent or catalytic binder removal system.

Powder metal parts typically require a thermal debind to remove some amount of “backbone” binder in a low temperature furnace followed by sintering in a high temperature furnace. For production needs some part manufacturers will utilize a low temperature belt furnace for thermal debind followed by sintering in a vacuum furnace or atmospheric continuous furnace. In the case of product development work, continuous furnaces are inflexible, they do not have the ability to work with a great variety of materials, and therefore batch vacuum furnaces are the better choice. Some vacuum furnaces have the ability to do both the thermal debind and sinter. This is advantageous because it minimizes handling losses and contamination issues while also eliminating process steps.

Batch vacuum furnaces can run a wide variety of product on any given day, making them especially attractive to short run, small volume, or product development work. This flexibility allows part producers to work with a wider variety of alloys, shapes, and binders to best develop highly technical parts.

Batch vacuum furnaces typically come with either graphite or refractory metal linings. Graphite linings are limited in processing characteristics in comparison to refractory metal. In a graphite furnace thermal debinding and sintering can only be done under a vacuum, up to a maximum of 5 Torr of hydrogen, or 15-30 Torr of nitrogen or argon. Processing at higher partial pressures can be dangerous from a methane formation standpoint as well as being very hard on the graphite itself. Graphite also has the tendency to hold binder material, in the form of carbon, and re-deposit this material on the parts during the sintering process. This makes carbon control and product uniformity difficult.

These limitations of a graphite furnace make a refractory metal furnace much more favorable. Refractory metal furnaces do not have any pressure limitations and can operate up to atmospheric pressure under hydrogen, nitrogen, argon, or any combination of those gasses as well as vacuum. This flexibility provides the perfect tool for both research and development and production that will vary from day to day or week to week.

 
DSH Technologies, LLC
107 Commerce Road
Cedar Grove , NJ 07009

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